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Transcription 1 Journal of Chromatography A, Review Recent applications of high-performance liquid chromatography to the analysis of metal complexes P.

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Wang, H. This paper reviews the most recent applications of high-performance liquid chromatography HPLC to the analysis of metal complexes.

The review centres on the use of the technique in metal complex syntheses, reactions, characterizations and complexations and retention behaviour of these compounds, as reported in the Amarina Sysdetector 4 since Amarina Sysdetector 4 Science B. Reviews; Metal complexes; Organometallic compounds Contents 1. Introduction Separation and determination HPLC separation and detection techniques Separation of isomers Studies on retention behaviour Applications to synthesis, reaction, characterization and complexation Conclusions References Introduction analytical and physical techniques.

Amongst these techniques, high-performance liquid chromatography Apart from their importance in the materials and HPLC is Amarina Sysdetector 4 used for the separation, determicatalysis areas, metal ions and their complexes play nation, and in the preparation of organometallic an important role in the vital functions of living compounds and metal coordination compounds. All rights reserved.

Table 1 summarizes many of the HPLC ficiency, and can be coupled to many sensitive and applications in the analysis of metal complexes from selective detectors.

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The first reported use of Amarina Sysdetector 4 to for the separation of organometallic complexes was Except for the widely used UV spectrophotometric made by Veening et al. Chromatographic detection primarily photodiode array detection, analysis of metal complexes carried out by tradition- PDAfluorescence detection has been used extenal gravity column chromatography CC and thin- sively for the detection of metal complexes.

After Amarina Sysdetector 4 these difficulties since the analysis is column reaction with lumogallion, the Al lumogallperformed rapidly under ambient temperature and the ion complexes were quantitated by fluorescence system stainless-steel columns, degassed mobile detection. In a considerable popularity in this field [2,3]. During the later work, a simple and sensitive HPLC method for past few years, the rapid developments of column quantifying aluminum in serum and urine by measurand an Amarina Sysdetector 4 variety of detection techniques ing the fluorescence of the Al lumogallion complex have made it suitable for the separation and de- was described [91].

Schuster and Sando [92] used termination of metal complexes. It does not ethylthiourea.

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Also presented were the first measurecover those applications carried by so-called ion ments of fluorescence decay times of the ligand as chromatography IC. We have limited the review to well as some complexes. Copper complexes with the work that involves the complexation of metals fulvic, caffeic, vanillic and salicylic acids Amarina Sysdetector 4 with ligands before injection into the HPLC Amarina Sysdetector 4.

Those ment and direct complex introduction methods [93].

In this method, free Gd was complexed analysing non-metal-species by complexing them with cyclohexanediaminetetraacetic acid CDTA with metal Amarina Sysdetector 4, are excluded from this review. Although spectrophotometric detection has been most popular, electrochemical, pulsed amperometric 2. Separation and determination and other detection methods have also been applied to metal complex analysis.

Weber [95] used triple HPLC separation and detection techniques step pulsed amperometry to detect selectively metal complex species after HPLC separation in the pres- In the field of metal complex analysis in the past ence of coeluting matrix compounds. The method is 3 P. Optimised pled plasma isotope-dilution mass spectrometry ICpulse parameters enable accurate and selective de- P-IDMS and particle beam mass spectrometry PBtection Amarina Sysdetector 4 some metal complexes even in the pres- MS are of increasing interest to analytical researchence of electroactive Amarina Sysdetector 4 such as phenols or ers.

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  • Recent applications of high-performance liquid chromatography to the analysis of metal complexes

The method has been applied to PB-MS technique was used in the elucidation of the the determination of vanadium v in two river water structure of polar organometallic compounds, such as samples and one mussel homogenate [96]. Yama- the chromium carbene complexes [99]. A HPLC moto et Amarina Sysdetector 4. Accurate results were obtained by the applicaamino acid copper ii complexes.

Rotational ICP-AES atomic emission spectrometry for the isomers of Amarina Sysdetector 4 group-6 metal tetracarbonyl complexdetermination of trace amounts of metallorganic es of 3,4-diphosphinidenecyclobutenes protected compounds in marine ecosystem has been reported with the 2,4-di-tert. Cairns et al. Nowotnik et al.

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Suzuki et al. Separation of enantiomers provided Se among biological constituents and its Amarina Sysdetector 4 HPLC needs specific conditions that differ from effect on endogenous Se in rats.

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Se, mono- separations of any other compounds. Recent admethylselenol and trimethylselenonium ion were vances in HPLC have made available several classes separated and detected. Ebdon et al. Amarina Sysdetector 4

Cole et al. Diastereomers of [RuCl 2 eta 6 - in the separation of technetium complexes. Linder tions, as shown in Table 2. RP-HPLC chromatographic data for five dihydropyridine calcium antago- Recent papers focusing on the analysis of the nists Cas were Amarina Sysdetector 4 on a b-cyclodextrin colisomers of the metal complexes include that by umn by Amarina Sysdetector 4 et al.

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